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ISSN: 2414-3146

April 2025 issue

Highlighted illustration

Cover illustration: The significant structural feature in the AgI complex (nitrito-κ2O:O′)bis­[tris­(4-fluoro­phen­yl)phosphine-κP]silver(I), [Ag(NO2)(C18H12F3P)2], is the small bite angle of the nitrito ligand [49.80 (5)°], which influences the overall geometry. See: Malan, Potgieter & Meijboom [IUCrData (2025). 8, x250296].

inorganic compounds


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The title single-crystal (icosa­magnesium dodeca­aluminium icosa­zinc), was obtained during the synthesis of an Mg–Al–Zn alloy at high pressure and temperature. There are significant difference between the current model and that of previous studies.

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A monoclinic ordered Mg9Ru2 phase with C2/c space-group symmetry rather than previously reported cubic Mg44Ru7 or Mg3Ru2 was obtained via high-pressure sinter­ing during the effort of synthesizing a target Mg—Ru—B compound.

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A CaCu1.424Fe0.576Si2 phase was obtained during high-pressure sinter­ing of an Si-rich quasicrystal composition prealloy with the nominal chemical com­position Si61Cu30Ca7Fe2. The obtained phase crystallizes in the space group I4/mmm (No. 139), with a = b = 4.041 Å and c = 10.010 Å.

metal-organic compounds


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The significant structural feature in the title AgI complex is the small bite angle of the nitrito ligand [49.80 (5)°], which influences the overall geometry.

organic compounds


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The crystal structure of a protonated Schiff base, isolated as its nitrate salt, exhibits a supra­molecular chain-like architecture that propagates along the crystallographic b-axis direction and features inter­molecular O—H⋯O and C—H⋯O hydrogen-bonding.


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A two-dimensional supra­molecular architecture mediated by N—H⋯N and N—H⋯O hydrogen bonds is formed in the crystal of the title compound.

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In the title compound, the pendant phenyl ring is twisted by 43.85 (1)° with respect to the acridine moiety. The extended structure features aromatic π–π stacking with a centroid-to-centroid distance of 3.489 (2) Å and weak C—H⋯O hydrogen bonds.

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In the title hydrate, the dihedral angle between the aromatic rings is 9.6 (3)°. In the crystal, N—H⋯O and O—H⋯N hydrogen bonds link the components into (101) sheets.

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The title compound, 3-chloro­propio­phenone C9H9ClO, consists of an almost planar mol­ecule that is charaterized by very small torsion angles within the alkyl side chain (torsion angles < 6.3°).
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