Figure 3
A single frame collected over 2° in ω over 1800 s for the plastic phase of cyclohexane at 245 K (bottom). Only the small part of the frame containing Bragg peaks is shown. The 3D plot of the frame (CBF format) was obtained using CAP Frame View v. 1.3 (Rigaku OD, 2015). Top inset: Reflection (1) rebuilt using 183 collected frames. The projection is normal to [0], with [100] running on the right and [01] running upward. This image was generated using X-AREA (Stoe & Cie, 2019). |