The crystal structures of 3-O-benzyl-1,2-O-iso­propyl­idene-5-O-methane­sulfonyl-6-O-tri­phenyl­methyl-α-d-gluco­furan­ose and its azide displacement product

Clarke, Z.; Barnes, E.; Prichard, K.L.; Mares, L.J.; Clegg, J.K.; McCluskey, A.; Houston, T.A.; Simone, M.I.

doi:10.1107/S205698901800765X

Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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Figure 1
The synthesis of the title compounds. Reagents and conditions. (i) trifluoromethanesulfonyl anhydride, DCM, pyridine, 243 K (to 2); methanesulfonyl chloride, DMAP, DCM, Et₃N (67%) (to 3); (ii) NaN₃, DMF, r.t. (88% over two steps from 1 via 2). The numbering system used is highlighted in red.

CRYSTALLOGRAPHIC
COMMUNICATIONS

ISSN: 2056-9890

Volume 74| Part 6| June 2018| Pages 862-867

https://doi.org/10.1107/S205698901800765X

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