forthcoming articles

The following articles are a selection of those recently accepted for publication in IUCrData.

See also Forthcoming articles in all IUCr journals.

Accepted 6 December 2019

Di­ethyl 4-(3-chloro­phen­yl)-2,6-di­phenyl-1,4-di­hydro­pyridine-3,5-di­carboxyl­ate

The di­hydro­pyridine ring adopts a shallow boat conformation. The mean plane of the di­hydro­pyridine ring (all atoms) subtends dihedral angles of 66.54 (1), 73.71 (1) and 79.47 (1)° with with the two phenyl rings and the chloro­phenyl ring, respectively. In the crystal, N—H⋯O hydrogen bonds link the mol­ecules into [001] chains.

Accepted 4 December 2019

6,6′-[(3,3′-Di-tert-butyl-5,5′-dimeth­oxy-1,1′-bi­phenyl-2,2′-di­yl)bis­(­oxy)]bis­(dibenzo[d,f][1,3,2]dioxaphosphepine) benzene monosolvate

The crystal structure of the benzene monosolvate of the well known organic diphosphite ligand C46H44O8P2 (BIPHEPHOS) is reported for the first time. Single crystals were obtained from a benzene solution after layering with n-heptane at room temperature.

Accepted 3 December 2019


The crystal structure of the title compound has been solved by single-crystal X-ray diffraction at 173 K. The crystals of the substance have been grown from the substances liquid phase at 277 K.

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