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Figure 4
Scheme of the apparatus used for the synthesis of NbF5. (a) Connection to a metal Schlenk line for evacuation, purging with inert gas, and fluorine supply, (b) tube furnace, (c) copper pipe surrounded by a heating sleeve, (d) PFA U-trap for product collection equipped with Monel connectors and diaphragm valves (Hoke), (e) PFA gas wash bottle with steel fitting filled with perfluoro polyether, (f) outlet connected to the absorber.

Journal logoCRYSTALLOGRAPHIC
COMMUNICATIONS
ISSN: 2056-9890
Volume 79| Part 12| December 2023| Pages 1207-1211
https://doi.org/10.1107/S2056989023010150
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